
Yang Fluidization, Solids Handling, and Processing
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FLUIDIZATION, SOLIDS HANDLING, AND PROCESSING
Industrial Applications
Edited by
Wen-Ching Yang
Siemens Westinghouse Power Corporation
Pittsburgh, Pennsylvania
np NOYES PUBLICATIONS
Westwood, New Jersey, U.S.A.
Copyright © 1998 by Noyes Publications
No part of this book may be reproduced or utilized in any form or by any means, electronic or mechanical, including photocopying, recording or by any information storage and retrieval system, without permission in writing from the Publisher.
Library of Congress Catalog Card Number: 98-18924 ISBN: 0-8155-1427-1
Printed in the United States
Published in the United States of America by Noyes Publications
369 Fairview Avenue, Westwood, New Jersey 07675 10 9 8 7 6 5 4 3 2 1
Library of Congress Cataloging-in-Publication Data
Fluidization, solids handling, and processing : industrial applications / edited by Wen-Ching Yang.
p . |
cm . |
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Includes bibliographical references and index. |
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ISBN 0 |
-8155 |
-1427-1 |
1. Fluidization. 2. Bulk solids flow. I. Yang, Wen-ching, 1939- |
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TP156.F65F5828 |
1998 |
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660 ' .284292 |
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PARTICLE TECHNOLOGY SERIES
Series Editor: Liang-Shih Fan, Ohio State University
FLUIDIZATION, SOLIDS HANDLING, AND PROCESSING: Edited by Wen-Ching Yang
INSTRUMENTATION FOR FLUID-PARTICLE FLOWS: by S. L. Soo
v

Contributors
John C. Chen |
Thomas B. Jones |
Department of Chemical |
Department of Electrical |
Engineering |
Engineering |
Lehigh University |
University of Rochester |
Bethlehem, PA |
Rochester, NY |
Bryan J. Ennis |
S.B. Reddy Karri |
E&G Associates |
Particulate Solid Research, Inc. |
Nashville, TN |
Chicago, IL |
Liang-Shih Fan |
George E. Klinzing |
Department of Chemical |
Department of Chemical and |
Engineering |
Petroleum Engineering |
Ohio State University |
University of Pittsburgh |
Columbus, OH |
Pittsburgh, PA |
Leon R. Glicksman |
Ted M. Knowlton |
Department of Architecture, |
Particulate Solid Research, Inc. |
Building Technology Program |
Chicago, IL |
Massachusetts Institute of |
|
Technology |
Mooson Kwauk |
Cambridge, MA |
Institute of Chemical Metallurgy |
|
Adacemia Sinica |
|
Beijing, People’s Republic of |
|
China |
ix
x |
Contributors |
|
JackReese |
Joachim Werther |
|
Department of Chemical |
Technical University Hamburg- |
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|
Engineering |
Harburg |
Ohio State University |
Hamburg, Germany |
|
Columbus, OH |
Peter Wypych |
|
|
|
|
Jens Reppenhagen |
Department of Mechanical |
|
Technical University Hamburg- |
Engineering |
|
|
Harburg |
University of Wollongong |
Hamburg, Germany |
Wollongong, NSW, Australia |
|
Ellen M. Silva |
Shang-Tian Yang |
|
Department of Chemical |
Department of Chemical |
|
|
Engineering |
Engineering |
Ohio State University |
Ohio State University |
|
Columbus, OH |
Columbus, OH |
|
Gabriel I. Tardos |
Wen-Ching Yang |
|
Department of Chemical |
Science and Technology Center |
|
|
Engineering |
Siemens Westinghouse Power |
City College of City University of |
Corporation |
|
|
New York |
Pittsburgh, PA |
New York, NY |
Frederick A. Zenz |
|
|
|
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Richard Turton |
Process Equipment Modeling & |
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Department of Chemical |
Mfg. Co., Inc. |
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Engineering |
Cold Spring, NY |
West Virginia University |
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Morgantown, WV |
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Preface
This volume, Fluidization, Solids Handling, and Processing, is the first of a series of volumes on “Particle Technology” to be published by Noyes Publications with L. S. Fan of Ohio State University as the consulting editor. Particles are important products of chemical process industries spanning the basic and specialty chemicals, agricultural products, pharmaceuticals, paints, dyestuffs and pigments, cement, ceramics, and electronic materials. Solids handling and processing technologies are thus essential to the operation and competitiveness of these industries. Fluidization technologyis employed not only in chemical production, it also is applied in coal gasification and combustion for power generation, mineral processing, food processing, soil washing and other related waste treatment, environmental remediation, and resource recovery processes. The FCC (Fluid Catalytic Cracking) technology commonly employed in the modern petroleum refineries is also based on the fluidization principles.
There are already many books published on the subjects of fluidization, solids handling, and processing. On first thought, I was skeptical about the wisdom and necessity of one more book on these subjects. On closer examination, however, I found that some industrially important subjects were either not covered in those books or were skimpily rendered. It would be a good service to the profession and the engineering community to assemble all these topics in one volume. In this book, I have invited recognized experts in their respective areas to provide a detailed treatment
vi
Preface vii
of those industrially important subjects. The subject areas covered in this book were selected based on two criteria: (i) the subjects are of industrial importance, and (ii) the subjects have not been covered extensively in books published to date.
The chapter on fluidized bed scaleup provides a stimulating approach to scale up fluidized beds. Although the scaleup issues are by no means resolved, the discussion improves the understanding of the issues and provides reassessments of current approaches. The pressure and temperature effects and heat transfer in fluidized beds are covered in separate chapters. They provide important information to quantify the effects of pressure and temperature. The gas distributor and plenum design, critical and always neglected in other books, are discussed in detail. For some applications, the conventional fluidized beds are not necessarily the best. Special design features can usually achieve the objective cheaper and be more forgiving. Two of the non-conventional fluidized beds,recirculating fluidized beds with a draft tube and jetting fluidized beds, are introduced and their design approaches discussed. Fluidized bed coating and granulation, applied primarily in the pharmaceutical industry, is treated from the fluidization and chemical engineering point of view. Attrition, which is critical in design and operation of fluidized beds and pneumatic transport lines, is discussed in detail in a separate chapter. Fluidization with no bubbles to minimize bypassing, bubbleless fluidization, points to potential areas of application of this technology. The industrial applications of the ever-increasingly important three-phase fluidization systems are included as well. The developments in dense phase conveying and in long distance pneumatic transport with pipe branching are treated separately in two chapters. The cyclone, the most common component employed in plants handling solids and often misunderstood, is elucidated by an experienced practitioner in the industry. The book is concluded with a discussion on electrostatics and dust explosion by an electrical engineer.
This book is not supposed to be all things to all engineers. The primary emphasis of the book is for industrial applications and the primary audience is expected to be the practitioners of the art of fluidization, solids handling, and processing. It will be particularly beneficial for engineers who operate or design plants where solids are handled, transported, and processed using fluidization technology. The book, however, can also be useful as a reference book for students, teachers, and managers who study particle technology, especially in the areas of application of fluidization technology and pneumatic transport.
viii Preface
I’d like to take this opportunity to thank Professor Fan who showed confidence in me to take up this task and was always supportive. I’d also like to thank the authors who contributed to this book despite their busy schedules. All of them are recognized and respected experts in the areas they wrote about. The most appreciation goes to my wife, Rae, who endured many missing weekends while I worked alone in the office.
Pittsburgh, Pennsylvania |
Wen-Ching Yang |
February, 1998 |
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NOTICE
To the best of our knowledge the information in this publication is accurate; however the Publisher does not assume any responsibility or liability for the accuracy or completeness of, or consequences arising from, such information. This book is intended for informational purposes only. Mention of trade names or commercial products does not constitute endorsement or recommendation for use by the Publisher. Final determination of the suitability of any information or product for use contemplated by any user, and the manner of that use, is the sole responsibility of the user. We recommend that anyone intending to rely on any recommendation of materials or procedures mentioned in this publication should satisfy himself as to such suitability, and that he can meet all applicable safety and health standards.

Contents
1 Fluidized Bed Scale-up .............................................................. |
1 |
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Leon R. Glicksman |
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1.0 |
INTRODUCTION .................................................................................... |
1 |
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2.0 |
REACTOR MODELING: BED DIAMETER INFLUENCE ............... |
4 |
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3.0 |
INFLUENCE OF BED DIAMETER ON HYDRODYNAMICS ....... |
10 |
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3.1 |
Bubbling Beds................................................................................. |
10 |
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3.2 |
Mixing ................................................................................... |
20 |
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3.3 |
Influence of Bed Diameter on Circulating Fluidized Beds .......... |
22 |
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3.4 |
Flow Transition ............................................................................... |
25 |
4.0 |
EXPERIMENTAL MEANS TO ACCOUNT FOR SCALE-UP: USE |
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OF SCALE MODELS ........................................................................... |
26 |
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4.1 |
Development of Scaling Parameters ............................................. |
27 |
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4.2 |
Governing Equations ...................................................................... |
29 |
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4.3 |
Fluid-Solid Forces .......................................................................... |
35 |
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4.4 |
Spouting and Slugging Beds .......................................................... |
38 |
5.0 |
SIMPLIFIED SCALING RELATIONSHIPS ...................................... |
39 |
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5.1 |
Low Reynolds Number .................................................................. |
39 |
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5.2 |
High Reynolds Numbers ................................................................ |
41 |
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5.3 |
Low Slip Velocity........................................................................... |
42 |
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5.4 |
General Case ................................................................................... |
43 |
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5.5 |
Range of Validity of Simplified Scaling ....................................... |
44 |
xi
xiiContents
6.0FURTHER SIMPLIFICATIONS IN THE SCALING
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RELATIONSHIP ................................................................................... |
51 |
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6.1 |
Viscous Limit .................................................................................. |
51 |
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6.2 |
Other Derivations for Circulating Fluidized Beds ........................ |
54 |
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6.3 |
Deterministic Chaos ....................................................................... |
55 |
7.0 |
DESIGN OF SCALE MODELS ........................................................... |
56 |
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7.1 |
Full Set of Scaling Relationships ................................................... |
56 |
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7.2 |
Design of Scale Models Using the Simplified Set |
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|
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of Scaling Relationships ................................................................. |
61 |
8.0 |
EXPERIMENTAL VERIFICATION OF SCALING LAWS FOR |
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BUBBLING BEDS ................................................................................ |
65 |
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8.1 |
Hydrodynamic Scaling of Bubbling Beds .................................... |
65 |
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8.2 |
Verification of Scaling Relationships for Bubbling |
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and Slugging Beds .......................................................................... |
69 |
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8.3 |
Verification of Scaling Laws for Spouting Beds .......................... |
75 |
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8.4 |
Verification of Scaling Relationships for Pressurized |
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Bubbling Beds ................................................................................. |
76 |
9.0 |
APPLICATIONS OF SCALING TO COMMERCIAL BUBBLING |
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FLUIDIZED BED UNITS ..................................................................... |
80 |
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10.0 |
HYDRODYNAMIC SCALING OF CIRCULATING BEDS ............ |
91 |
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11.0 |
CONCLUSIONS ................................................................................. |
100 |
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ACKNOWLEDGMENTS ........................................................................... |
102 |
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NOTATIONS ................................................................................. |
103 |
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REFERENCES ................................................................................. |
104 |
2 Pressure and Temperature Effects in |
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Fluid-Particle Systems .......................................................... |
111 |
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Ted M. Knowlton |
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1.0 INTRODUCTION ................................................................................ |
111 |
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1.1 |
Minimum Fluidization Velocity .................................................. |
113 |
1.2 |
Bed Voidage and Bed Expansion ................................................ |
120 |
1.3 |
Bubbles in Fluidized Beds ........................................................... |
124 |
1.4 |
Bubble Size and Frequency ......................................................... |
125 |
1.5 |
Bed-to-Surface Heat Transfer Coefficient .................................. |
129 |
1.6 |
Entrainment and Transport Disengaging Height ........................ |
131 |
1.7 |
Particle Attrition at Grids ............................................................. |
134 |
1.8 |
Particle Attrition in Cyclones ....................................................... |
136 |
1.9 |
Jet Penetration ............................................................................... |
137 |
1.10 |
Regime Transitions ....................................................................... |
139 |
1.11 |
Cyclone Efficiency ....................................................................... |
146 |
NOTATIONS ................................................................................. |
147 |
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REFERENCES ................................................................................. |
149 |