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20. Apparatus

Having now covered the theory, we can start with the practical operations for actually making the

Philosophers' Stone. You first need to obtain the necessary apparatus.

For the First Part you will need two 500ml retorts for distilling the urine. It is important that this be a retort,

and not some modern distillation apparatus. The reason for this is that you are only distilling on low-heat, so

as not to destroy the life-energy. If you try to use modern distillation apparatus then the water vapor will not

rise high enough to escape before it condenses. The reason for the second retort is because you may have to

break the first one in order to extract the white salt, and also because the distilled urine will need to be

further distilled in a clean retort before moving on to the Second Part.

Update: it has been discovered by members of The Book of Aquarius forum that an alembic will distill the

urine up to 4x faster than a retort, though I do not have personal experience with an alembic. An alembic is

a dome-shaped vessel with a long downwards-pointing next which sits on top of a large round-bottom flask.

To use an alembic instead of a retort you will need two 500ml round-bottom flasks and one alembic. Make

sure that the size of the connections between the alembic and flasks are compatible. The instructions are

exactly the same whether you use a retort or an alembic, but for the calcinations you can remove the

alembic and only calcine the 500ml flask containing what is left of the urine after distillation.

You will need a 500ml glass bottle for collecting and storing the distilled urine.

For the Second Part, you will need a round-bottom flask in either Kjeldahl, Florence or boiling flask style.

The size you will need will likely be 50ml, depending on how much of the body you will be using. Try to

find one with a long neck. You can use one with a shorter neck, but for this you will have to make sure the

ambient (room) temperature is low enough for the water vapor to condense closer to the heat source.

The Kjeldahl flask has an egg-shaped bottom and a long neck, which is perfect for our purpose of imitating

the water cycle through evaporation and condensation, but even a normal boiling flask will do the job as

long as it has a round bottom. Do not use a flat-bottom flask.

You will need a pipette for accurately transferring the distilled urine into the flask.

You will need stoppers for sealing the flask.

For both parts you will need a water bath, with digital temperature control. A water bath is the best heat

source, since the water is all at an even temperature, the lower part of the flask can be immersed in the

water, and the temperature can be adjusted very precisely. Get the smallest one you can, it needs only be

large enough for the 500ml retort.

You will also need a dry heat source for calcining the retort between distillations. You could do this on a

portable gas stove or electric hot plate. Or you could purchase a lab-grade heating mantle, which is more

expensive but much easier to use. The calcining will need to be done outside, so you will not be able to use

your kitchen stove.

You will need a support stand (I recommend a triangle stand), with the clamp attachments for holding the

retort or flask in place over the water bath.

If you can afford it, get 2 (or more) of everything, just in case. It's also a good idea to get a collection of

various bottles, spatulas, stoppers, dishes, mortar and pestle, and other fun things like that, which are not

absolutely necessary, but will certainly be very useful. Otherwise you'll have to improvise with what you

can find in the kitchen.

The glassware (retort and flask) should be made of borosilicate glass, which is pretty much standard these

days, so it should not be much trouble to find. Borosilicate glass can stand very high heat without cracking.

If you buy the water bath or other electrical items from abroad, be sure to check it works on the same

voltage as in your country. If not you will need to buy a voltage converter as well. If you plug a 110V

appliance into a 220V supply you could end up burning down your house, so do pay attention to this.

The water bath will need to be running 24/7, so if you live in an area with frequent power cuts I

recommend getting a backup generator.

Checklist (minimum):

1. 2x retort, 500ml (or 1x alembic + 2x round-bottom flask, 500ml)

2. Glass bottle, 500ml

3. Round-bottom flask, 50ml

4. Pipette

5. Stoppers

6. Water bath

7. Portable stove or heating mantle

8. Support stand

The following quote is a description of the vessel to be used for the Second Part of the Work.

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The vessel for our stone is but one, in which the whole magistery or elixir is performed and perfected; this is a

cucurbit, hose bottom is round like an egg, or an urinal, smooth within, that it may ascend and descend the more

easily, covered with a limbeck round and smooth every where, and not very high, and whose bottom is round also like

an egg. Its largeness ought to be such, that the medicine or matter may not fill above a fourth part of it, made of strong

durable glass, clear and transparent, that you may see through it, all the colours appertaining to, and appearing in

the work; in which the spirit moving continually, cannot pass or fly away. Let it also be so closed, that as nothing can

go out of it, so nothing can enter into it; [...] And though the philosophers oftentimes say, that the matter is to be put

into the vessel, and closed up fast, yet it is sufficient for the operator, once to put the said matter in, once to close it up,

and so to keep it even to the very perfection and finishing of the work.

The Root of the World, by Roger Bacon, 13th Cen.

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-

21. First Part

Collect 500ml of urine, the darker the better, so it's best to collect it from the first time you urinate in the

morning. If you don't get enough then you can top it up during the day, or wait until the next morning.

Don't leave the urine in an open container.

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it [the urine] must be purged of its watery and earthy nature (for at first it appears an earthy, heavy, thick, slimy, and

misty body), and all that is thick, nebulous, opaque, and dark in it must be removed, that thus, by a final sublimation,

the heart and inner soul contained in it may be separated and reduced to a precious essence.

The Sophic Hydrolith, Or, Water Stone of the Wise, by Anonymous, 17th Cen.

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Distil the urine at no more than 175°F/80°C in the water bath with the retort. It should take 1-2 weeks to

distil the urine once. Obviously the distillation will be faster if the ambient (room) temperature is lower

(though not below freezing). The top opening of the retort should be hermetically sealed.

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