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Analytes Methods Matrix

Greenness

assessment (GA) Solvent

Year and

window (W) References

Paracetamol,

aceclofenac, and thiocolchicoside

Simultaneous equation Tablet formulation GA Phosphate

buffer pH 7.8

2021

[139]

Sofosbuvir and velpatasvir Second derivative ratio spectra Epclusa tablets GA Methanol 2021

[140]

Dacarbazine and its related

impurities

Double dual wavelength

Dual ratio subtraction

Successive ratio subtraction

Dacarbazine

medac® powder for

injection

None Methanol for

stock solution

and water for

working

solution

2021

[141]

Sulfasalazine and its related

compounds

Modified ratio difference

Mean centring

Colosalazine-ECVR

and

Marsalaz VR tablets

GA Acetone

diluted with

ethanol

2021

[142]

Flumethasone pivalate and

clioquinol

Dual wavelength

Fourier self-deconvolution

First derivative ratio spectra

Bivariate procedures

Area under the curve

Combined

formulation

Viotic VR ear drops

None Methanol 2021

[143]

Miconazole nitrate and nystatin Dual wavelength

Absorption correction

Ratio difference

First derivative ratio spectra

Mean centring

Ratio subtraction

Combined

suppositories and

dissolution testing

None Methanol for

working

standard

solution

Bi-distilled water

for inv itro

dissolution

2021

[144]

(Continued)

https://t.me/medicina_free

Analytes Methods Matrix

Greenness

assessment (GA) Solvent

Year and

window (W) References

Azithromycin and levofloxacin First derivative Laboratory-

prepared tablets

GA Methanol 2020

[145]

Mebendazole and quinfamide Extended ratio subtraction

coupled with isoabsorptive point

Dual wavelength

Simultaneous ratio subtraction

Absorbance subtraction

Vermox Plus®

tablets

None Methanol 2020

[146]

Acefylline piperazine and

bromhexine hydrochloride

Dual wavelength within the ratio

spectra

Double divider-ratio spectra

derivative

Mucophylline®

syrup

None Methanol 2020

[147]

Alfuzosin and solifenacin Dual wavelength

Determination in zero order

First derivative ratio spectra

Derivative ratio

Ratio difference

Mean centring

Solitral® capsules GA Water 2020

[148]

Zofenopril calcium and

hydrochlorothiazide

Absorbance subtraction

Ratio subtraction linked to

constant multiplication

Advanced amplitude modulation

Ratio difference

Zoprotec Plus®

film-coated tablets

None Methanol 2020

[123]

Table 8.4 (Continued)

https://t.me/medicina_free

Analytes Methods Matrix

Greenness

assessment (GA) Solvent

Year and

window (W) References

Sulfadimidinesodium,

sulfaquinoxaline sodium,

diaveridine, and vitamin K

Amplitude modulation

Successive ratio subtraction

linked to constant multiplication

Absorbance subtraction

Coccimix® powder

veterinary

formulation

None Water 2020

[149]

Ciprofloxacin hydrochloride and

metronidazole

Continuous wavelet transform Ciprodiazole tablets None Acidic pH

monitoring

solution (0,1 M)

HCl with pH 1.2

2020

[150]

Cetylpyridinium chloride and

lidocaine hydrochloride with

dimethylaniline

Ratio difference

First derivative ratio spectra

Dual wavelength linked to the

isoabsorptive point

Dentinox® teething

gel

None Distilled water 2020

[151]

Ranitidine hydrochloride and

metronidazole

Response correlation

Absorptivity centring

Flagyl® 500 mg and

Zantac® 150 mg

None Methanol 2020

[152]

Paracetamol, ibuprofen, and

caffeine

Continuous wavelet transform Bidi-Ipalvic

capsules and

Glotasic tablets

Dissolution profiles

None Phosphate

buffer pH 7.8

2020

[153]

Diphenhydramine, paracetamol,

p-aminophenol and

diphenofydramine degraded

(N-oxide)

Dual wavelength

Three divider ratio difference

Double divider ratio difference

Quaternary

mixtures prepared

in a lab

Panadol night®

tablets for

quantitative

determination of

diphenhydramine

and paracetamol

None Methanol 2020

[154]

(Continued)

https://t.me/medicina_free

Analytes Methods Matrix

Greenness

assessment (GA) Solvent

Year and

window (W) References

Clioquinol,

betamethasone tolnaftate,

gentamicin and preservative

chlorocresol

Constant value spectrum

subtraction

Constant multiplication

Derivative ratio

Concentration value

Factorised derived ratio linked to

spectrum subtraction

Quadriderm cream None Stock solutions

in methanol,

except for

gentamicin in

bi-distilled

water

2020

[127]

Alogliptin and pioglitazone Induced amplitude modulation

Induced concentration

subtraction

Induced dual wavelength

Oseni® tablets None Methanol 2020

[27]

Tylosin tartrate and doxycycline

hydrochloride

Absorbance subtraction

Amplitude summation

Ratio subtraction linked to

extended ratio subtraction

Spectrum subtraction

Successive derivative subtraction

Concentration value

Constant value

Derivative transformation

Direct spectrophotometry

Successive derivative subtraction

linked to spectrum subtraction

Derivative subtraction linked to

constant multiplication

Tydovet® powder

veterinary medicine

None Methanol 2020

[20, 70,

72, 73, 75,

84]

Table 8.4 (Continued)

https://t.me/medicina_free

Analytes Methods Matrix

Greenness

assessment (GA) Solvent

Year and

window (W) References

Cangliflozin and metformin Absorbance difference

Absorbance at isoabsorptive

point

Amplitude at isosbestic point

Vokanamet® tablets GA Methanol 2020

[122]

Tylosin tartrate and doxycycline

hydrochloride

Induced dual wavelength

Dual wavelength

Absorption correction

Absorbance subtraction

Amplitude correction

Derivative ratio

Advanced amplitude modulation

Tydovet® powder

veterinary medicine

None Methanol 2020

[24]

Ciprofloxacin and acidic degraded

(chloro analogue)

Pure component contribution

algorithm

CEPROZ® tablets None Methanol 2020

[155]

Metoclopramide and aspirin

(acetyl salicylic acid)

Ratio H-point standard addition

Absorptivity centring

Geometrically induced amplitude

modulation

Migramax sachets None Water :

methanol (50 :

50 v/v)

2020

[101]

Dapagliflozin and saxagliptin Factorised zero order derivative

Ratio difference

In-house

formulation of

Qtern® tablets

None Methanol 2019

[156]

Amlodipine besylate and

rosuvastatin calcium

Induced dual wavelength

Amplitude correction

Absorbance subtraction

Absorption correction

Advanced amplitude subtraction

Rosucor® Plus

film-coated tablets

None Methanol 2019

[157]

(Continued)

https://t.me/medicina_free

Analytes Methods Matrix

Greenness

assessment (GA) Solvent

Year and

window (W) References

Ofloxacin and dexamethasone Absorptivity centring

Absorbance subtraction

Amplitude modulation

Amplitude summation

Dexaflox® eye drops None Ethanol : water

(50 : 50 v/v)

2019

[121]

Pseudoephedrine sulfate and

loratadine

Induced amplitude modulation

Ratio difference

Absorption correction

Dual wavelength

Direct analysis

Constant multiplication

Induced dual wavelength

Clarinase® tablets None 0.1 M HCl 2019

[25]

Ciprofloxacin and fluocinolone

acetonide

Absorptivity centring

Extended ratio subtraction

Constant multiplication

Unified constant subtraction

Spectrum subtraction

Ratio subtraction

Otovel® otic

solution

None Methanol 2019

[82, 84]

Phenazone and

benzocaine

Absorptivity centring

Absorbance subtraction

Amplitude modulation

Concentration value

Tympanil® otic

drops

None Ethanol 2019

[75, 158]

Table 8.4

(Continued)

https://t.me/medicina_free

Analytes Methods Matrix

Greenness

assessment (GA) Solvent

Year and

window (W) References

Ciprofloxacin and fluocinolone

acetonide

Isoabsorptive point coupled with

direct spectrophotometry

Isoabsorptive point linked to area

under the curve

Isoabsorptive point coupled with

amplitude modulation

Otovel® otic

solution

None Methanol 2019

[159]

Metformin hydrochloride,

empagliflozine, linagliptin and

pioglitazone hydrochloride

Mean centring

Ratio derivative–zero crossing

Glucophage®,

Jardiance®,

Trajenta® and

Actos® tablets

None Methanol 2019

[160]

Trimebutine maleate with

degradation product (DEG) 1

(3,4,5-trimethoxy benzoic acid)

and DEG 2 (2-dimethyl amino)-2

phenyl butanol

Dual wavelength

Second derivative ratio spectra

Ratio difference

Constant centre linked to

spectrum subtraction

Gast-reg® tablets,

ampoules, and

suspension

None Methanol 2019

[161]

Aceclofenac and paracetamol with

degraded diclofenac sodium and

4-minophenol

Dual wavelength

Induced dual wavelength

Unlimited derivative

Successive derivative subtraction

linked to constant multiplication

Ratio difference

Constant centre

Hifenac-P® tablets None Methanol 2019

[126]

Daclatasvir, sofosbuvi and

ribavirin

Pure component contribution

algorithm

Daklanork® tablets None Methanol 2019

[162]

Ciprofloxacin and metronidazole Pure component contribution

algorithm

Ciprodiazole®

tablets

None Distilled water 2019

[115]

(Continued)

https://t.me/medicina_free

Analytes Methods Matrix

Greenness

assessment (GA) Solvent

Year and

window (W) References

Thioctic acid, benfotiamine and

cyanocobalamin

First derivative Ratio difference

First derived ratio spectra

Ratio subtraction

Thiotacid®

compound capsules

None Acetonitril :

water (50 : 50

v/v)

2019

[163]

Hydrochlorothiazide and

telmisartan

Q-absorbance ratio Micardis Plus® GA Methanol 2019

[164]

Pseudoephedrine hydrochloride

and ibuprofen

Dual wavelength

Ratio difference

Constant multiplication linked to

spectrum subtraction

Absorption correction

Constant centre linked to

spectrum subtraction

Brufen-Flu® tablets None Methanol 2019

[31]

Salbutamol, theophylline, and

ambroxol

Simultaneous equation

(Vierordt’s method)

Ambrolite-ST

tablets

None Methanol 2018

[165]

Chloramphenicol and

dexamethasone sodium phosphate

Ratio subtraction

Unified constant subtraction

Extended ratio subtraction

Constant multiplication

Spectrum subtraction

Spersadex® eye

drops

None Ethanol : water

(50 : 50 v/v)

2018

[84]

Ambroxol, fuaifenesin and

theophylline

Direct spectrophotometry

Dual wavelength

First derivative ratio spectra

Absorption correction

Trisolvin® capsules None Methanol 2018

[166]

Table 8.4 (Continued)

https://t.me/medicina_free

Analytes Methods Matrix

Greenness

assessment (GA) Solvent

Year and

window (W) References

Clotrimazole and dexamethasone

acetate

Constant centre

Constant value with amplitude

difference

Ratio difference

Advanced concentration value

Derived ratio spectra

Mycuten-D cream None Methanol 2018

[75, 167]

Carbinoxamine maleate,

pholcodine and ephedrine

hydrochloride

Successive derived ratio spectra

Successive derivative subtraction

coupled with constant

multiplication

Ratio subtraction linked to ratio

difference Amplitude summation

Continuous wavelet transform

Cyrinol syrup None Distilled water 2018

[70]

Paracetamol, chlorzoxazone and

diclofenac potassium

Continuous wavelet transform Myospazfort® tablet None Methanol 2018

[168]

Paracetamol, pseudoephedrine

hydrochloride and cetirizine

dihydrochloride

Ratio subtraction linked to ratio

difference

Derived ratio spectra linked to

zero crossing

Successive derivative ratio

Pure component contribution

algorithm

Allercet Cold®

capsules

None Distilled water 2018

[169]

(Continued)

https://t.me/medicina_free

Analytes Methods Matrix

Greenness

assessment (GA) Solvent

Year and

window (W) References

Ketorolac tromethamine,

phenylephrine hydrochloride and

chlorpheniramine maleate

First derivative ratio spectra

Derivative ratio

Difference ratio

Delta absorbance

Convolution of derived data by

discrete Fourier functions

MIDRIA® and

KETO-PC® eye

drops

None Distilled water 2018

[170]

Furosemide spironolactone and

canrenone

Successive ratio subtraction Lasilactone® tablets None Methanol 2018

[171]

Guaifenesin chlorpheniramine

and pseudoephedrine

Continuous wavelet transform Commercial cough

syrup

None Distilled water 2018

[172]

Chlorzoxazone and ibuprofen Amplitude modulation

Amplitude summation

Absorbance subtraction

Markfast® and

Profenazone®

capsules

None Ethanol : water

(50 : 50 v/v)

2018

[95]

Mix 1: Simvastatin and ezetimibe

Mix 2: Chloramphenicol and

prednisolone acetate

Absorptivity centring Inegy® tablets and

Cortiphen® eye

drops

None Methanol for

mix 1

Ethanol for mix

2018

[173]

Clotrimazole and dexamethasone Mean centring Mycuten-D® cream None Methanol 2018

[174]

Albendazole with alkaline

degraded substance

Derivative ratio Bendax® tablets None Methanol 2018

[175]

Table 8.4 (Continued)

https://t.me/medicina_free

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